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Adenosine monophosphate

Adenosine monophosphate (AMP), also known as 5'-adenylic acid, is a ribonucleoside 5'-monophosphate consisting of the nitrogenous base attached to a sugar, with a single group esterified at the 5' position of the ribose; its molecular formula is C10H14N5O7P and molecular weight is 347.22 g/mol. As a fundamental , AMP serves as a building block in ribonucleic acid (), where it contributes to the genetic information storage and protein synthesis processes. It also functions as a key metabolite in cellular , signaling low energy states by accumulating when (ATP) is hydrolyzed, thereby activating (AMPK) to promote catabolic pathways and inhibit anabolic ones for energy restoration. Beyond its structural role in nucleic acids, AMP participates in various biochemical pathways as a cofactor and ; for instance, it modulates activities, such as inhibiting fructose-1,6-bisphosphatase in . In immune function, AMP influences responses by reversing malnutrition-induced and supporting pools essential for proliferation. Additionally, cyclic AMP (cAMP), which is synthesized from ATP and degraded to AMP, is a critical second messenger in that regulates processes like hormone action, , and . Its dysregulation is implicated in metabolic disorders, including and cancer, highlighting its broader physiological significance.

Chemical structure and properties

Molecular composition

Adenosine monophosphate (AMP), also known as 5'-adenylic acid, is a monophosphate composed of the base , the sugar , and a single group esterified to the 5' carbon of the ribose. The is linked to the C1' anomeric carbon of the via a β-N9-glycosidic bond, forming the , to which the is attached through a phosphoester linkage. The molecular formula of AMP is C₁₀H₁₄N₅O₇P, and its IUPAC name is [(2R,3S,4R,5R)-5-(6-aminopurin-9-yl)-3,4-dihydroxyoxolan-2-yl]methyl dihydrogen . The structure features a planar ring system in (a fused and ring with an amino group at position 6), a five-membered ring in the (with hydroxyl groups at C2' and C3'), and the dihydrogen phosphate group (-OPO₃H₂) connected to the CH₂OH at C5' of the . AMP differs from related adenine nucleotides in the number of phosphate groups: adenosine diphosphate (ADP) has two phosphates linked by a phosphoanhydride bond (formula C₁₀H₁₅N₅O₁₀P₂), while adenosine triphosphate (ATP) has three (formula C₁₀H₁₆N₅O₁₃P₃), with the additional phosphates attached via high-energy phosphoanhydride bonds to the terminal phosphate of AMP. This monophosphate configuration positions AMP as a key intermediate in cellular energy transfer and signaling processes.

Physical and chemical characteristics

Adenosine monophosphate () appears as a white crystalline powder at . Its is 347.22 g/, calculated from its molecular formula C₁₀H₁₄N₅O₇P. The is approximately 2.32 g/mL, as determined by computational prediction based on molecular structure. AMP decomposes upon heating, with a range of 196–200 °C. AMP exhibits high solubility in water, approximately 10 g/L at 20 °C, attributable to the polar phosphate group that facilitates hydrogen bonding and ionization in aqueous environments. This solubility is enhanced under mildly alkaline conditions. The compound possesses three ionizable groups with approximate pKa values: pKa₁ ≈ 0.9 for the first dissociation of the phosphate (PO₄H₂/PO₄H⁻), pKa₂ ≈ 3.9 for the protonated adenine ring (N₁H⁺/N₁), and pKa₃ ≈ 6.0 for the second phosphate dissociation (PO₄H⁻/PO₄²⁻). These pKa values influence its reactivity and charge state at physiological pH, where AMP predominantly exists as a dianion. Chemically, is relatively stable under neutral conditions but undergoes of the bond in acidic or basic media, leading to cleavage into and inorganic . The group plays a key role in this reactivity, as its modulates nucleophilic attack and during . The moiety contributes to , with a characteristic UV absorption maximum at 257 nm, useful for spectrophotometric quantification.

and

Synthesis pathways

Adenosine monophosphate () is primarily synthesized in cells through and salvage pathways, as well as via enzymatic reactions involving . In synthesis, the pathway begins with 5-phosphoribosyl-1-pyrophosphate (PRPP), which is converted through a series of 10 enzymatic steps into inosine monophosphate (). then serves as the immediate precursor to , with adenylosuccinate synthetase catalyzing the GTP-dependent addition of aspartate to , forming adenylosuccinate. Subsequently, adenylosuccinate lyase cleaves fumarate from adenylosuccinate to yield . This branch of the pathway is energy-intensive, requiring contributions from such as , , and aspartate, along with one-carbon units and CO₂, and occurs primarily in the of tissues like the liver. The salvage pathway recycles free adenine bases, conserving energy compared to . Adenine phosphoribosyltransferase (APRT) catalyzes the transfer of the phosphoribosyl group from PRPP to , directly forming AMP in a single-step reaction. This enzyme is widely distributed and plays a key role in purine homeostasis by incorporating from dietary sources or metabolism. AMP can also be generated through energy-related reactions within the adenine nucleotide pool. The adenylate kinase reaction equilibrates ADP, ATP, and AMP via the reversible phosphorylation:
$2 \text{ADP} \rightleftharpoons \text{ATP} + \text{AMP}
with an apparent equilibrium constant K = \frac{[\text{ATP}][\text{AMP}]}{[\text{ADP}]^2} \approx 0.44 under physiological magnesium and pH conditions. This reaction maintains the balance of the adenine nucleotide pool during metabolic shifts, such as ATP depletion. Additionally, certain nucleotidases, including ectonucleotide pyrophosphatase/phosphodiesterase 1 (ENPP1), hydrolyze ATP directly to AMP and pyrophosphate (PPi):
\text{ATP} + \text{H}_2\text{O} \rightarrow \text{AMP} + \text{PP}_\text{i}
contributing to extracellular nucleotide regulation.
For research and industrial purposes, AMP is chemically synthesized by phosphorylating using (POCl₃) in the presence of , followed by purification to yield the 5'-monophosphate. Enzymatic methods, such as those employing kinases with ATP analogs, offer milder alternatives for producing modified AMP variants.

Degradation processes

Adenosine monophosphate (AMP) undergoes degradation primarily through two initial enzymatic pathways in cellular : and . is catalyzed by , which converts AMP to and inorganic (Pi), facilitating the release of the nucleoside for further processing or salvage. This reaction occurs in the and contributes to maintaining nucleotide pools under varying energy demands. The pathway involves AMP deaminase, which transforms into monophosphate () and (NH₃) as part of the purine nucleotide cycle, a process particularly active in to support and release during contraction. The purine nucleotide cycle includes subsequent steps where is converted to adenylosuccinate by adenylosuccinate synthetase and then back to by adenylosuccinate lyase, enabling the net release of from aspartate while regenerating . The key reaction is: \text{AMP} + \text{H}_2\text{O} \rightarrow [\text{IMP}](/page/Imp) + \text{NH}_3 This cycle aids in buffering changes and providing fumarate for the . Further of degradation products proceeds via salvage and breakdown routes. produced from is deaminated to by , while can be dephosphorylated to ; both inosines are then converted to hypoxanthine by phosphorylase. Hypoxanthine is oxidized to and subsequently to by , marking the end of the purine degradation pathway. Degradation of AMP is regulated by cellular energy status, with AMP deaminase activity increasing during energy depletion to promote ammonia production and nucleotide recycling. This process is also enhanced under hypoxic conditions, as observed in skeletal muscle where hypoxia stimulates ammonia output via the purine nucleotide cycle to adapt to reduced oxygen availability. In humans, uric acid serves as the primary excretory end product of purine catabolism, with dysregulation leading to hyperuricemia and conditions such as gout due to urate crystal deposition.

Physiological functions

Role in energy metabolism

Adenosine monophosphate (AMP) serves as a critical intracellular marker of low cellular status, where an elevated AMP/ATP ratio indicates ATP depletion under conditions of metabolic stress, such as intense exercise or starvation. This ratio shifts dynamically in response to energy demands, reflecting the cell's need to prioritize ATP regeneration over other processes. AMP participates in the adenine nucleotide pool alongside ATP and ADP, facilitating their interconversion through enzymatic reactions that preserve the overall energy charge of the cell. The energy charge, a key metric of metabolic poise, is quantified by the formula: \text{Energy charge} = \frac{[\text{ATP}] + 0.5[\text{ADP}]}{[\text{ATP}] + [\text{ADP}] + [\text{AMP}]} This index, originally proposed by Atkinson, typically ranges from 0.8 to 0.95 in healthy s, ensuring efficient by modulating enzymatic activities based on nucleotide balances. In , AMP acts as an allosteric activator of phosphofructokinase-1 (PFK-1), the rate-limiting enzyme that converts fructose-6-phosphate to fructose-1,6-bisphosphate, thereby accelerating glycolytic flux to boost ATP production. Similarly, AMP allosterically stimulates , promoting breakdown to glucose-1-phosphate and fueling rapid energy mobilization during demand. AMP is predominantly intracellular and maintains low basal levels under normal conditions, but its concentration rises notably in mitochondria during uncoupling events, where proton leak across the inner dissipates the without ATP , leading to heightened AMP/ATP ratios. This localization underscores AMP's role in coordinating mitochondrial responses to energy imbalances. The function of AMP in energy sensing exhibits remarkable evolutionary conservation, operating universally across prokaryotes and eukaryotes to link status with metabolic adaptation.

Regulatory roles including AMPK activation

Adenosine monophosphate (AMP) serves as a critical signaling in cellular energy regulation, primarily through its role as an allosteric activator of (AMPK), a heterotrimeric complex consisting of α, β, and γ subunits. AMP binds to the γ-subunit at its four cystathionine-β-synthase () domains, with preferential occupancy at site 3 and site 4, inducing conformational changes that enhance AMPK's catalytic activity. This binding promotes phosphorylation of the activation loop Thr172 residue on the α-subunit by upstream such as LKB1 (liver kinase B1) or CaMKKβ (Ca²⁺/calmodulin-dependent protein kinase kinase-β), while also inhibiting by protein phosphatase 2C (PP2C). Additionally, AMP facilitates autophosphorylation at Ser108 on the β-subunit, contributing to overall kinase stabilization and activity. These mechanisms collectively amplify AMPK up to 1000-fold in response to energy depletion.00356-6) The threshold of AMPK is highly sensitive to the AMP/ATP ratio, which rises during metabolic stress when exceeds production, converting ATP to ADP and then AMP via (2ADP ⇌ AMP + ATP). Basal cellular AMP/ATP ratios are approximately 0.01, but becomes significant when this ratio increases to 0.1 or higher, reflecting a 10-fold rise in AMP levels. Allosteric by AMP provides a ~5-fold increase in activity, while enhancement of Thr172 yields another ~10-fold boost, and inhibition of adds a further ~10-fold effect, with the net result scaling nonlinearly with the AMP/ATP ratio. This ultrasensitive response ensures AMPK acts as an effective energy sensor, prioritizing ATP conservation.00356-6)30396-9) Upon activation, AMPK phosphorylates downstream targets to restore energy balance, including (ACC), which inhibits by reducing production, thereby promoting fatty acid oxidation. AMPK also activates peroxisome proliferator-activated receptor γ coactivator 1α (PGC-1α), stimulating and oxidative metabolism to enhance ATP generation. In physiological contexts, activated AMPK in the liver suppresses by phosphorylating and inhibiting transcription factors like CREB-regulated transcription coactivator 2 (CRTC2), conserving glucose during or exercise. In skeletal muscle, AMPK promotes glucose uptake by facilitating translocation to the plasma membrane, supporting energy replenishment.00090-4)30396-9) Dysregulation of AMP-AMPK signaling contributes to pathological conditions like , characterized by , , and , where reduced AMPK activity impairs . Pharmacological agents such as metformin, a first-line treatment for , mimic AMP effects by inhibiting mitochondrial complex I, elevating the AMP/ATP ratio, and thereby activating AMPK to improve glucose handling and lipid metabolism.00090-4)

Connection to cyclic AMP

Cyclic adenosine monophosphate (cAMP) is a key second messenger in pathways, synthesized from ATP by , while AMP serves primarily in . cAMP enables rapid, transient communication between extracellular signals and intracellular responses, linking the two through shared biochemical intermediates. cAMP is synthesized from ATP by the membrane-bound enzyme , which is stimulated by G-protein-coupled receptors upon binding of hormones like or epinephrine; this process does not involve direct conversion from AMP. However, AMP indirectly connects to cAMP regulation as the primary product of cAMP , forming a loop that modulates signaling duration. The structure of cAMP consists of an molecule with a 3',5'-cyclic bond on the ring, giving it the molecular formula \ce{C10H12N5O6P}. In cellular signaling, cAMP binds to and activates protein kinase A (PKA), a tetrameric enzyme that dissociates into regulatory and catalytic subunits, allowing the catalytic subunits to phosphorylate target proteins and initiate downstream cascades. A prominent example is in hepatic cells, where glucagon elevates cAMP levels, activating PKA to phosphorylate enzymes such as phosphorylase kinase, which in turn promotes glycogen breakdown (glycogenolysis) to release glucose into the bloodstream. The duration of cAMP-mediated signaling is tightly controlled by cyclic nucleotide phosphodiesterases (PDEs), a family of enzymes that hydrolyze the 3',5'-phosphodiester bond of cAMP to yield 5'-AMP, thereby terminating the signal and recycling AMP for other metabolic uses. This degradation step closes the regulatory cycle between cAMP and AMP, ensuring precise spatiotemporal control of cellular responses. The concept of as a second messenger was discovered by Earl W. Sutherland in during studies on epinephrine's effects on , earning him the in or in 1971 for elucidating this fundamental mechanism of hormonal action. In contrast to the steady-state, energy-buffering role of linear AMP in processes like ATP regeneration, the cyclic configuration of facilitates its high-affinity binding to effectors like , enabling ephemeral bursts of activity suited to dynamic signaling rather than sustained metabolic maintenance.

Clinical and research applications

Therapeutic uses

Adenosine, derived from the dephosphorylation of (), is widely used in diagnostic cardiac to induce coronary , facilitating in patients unable to exercise. This pharmacologic stress agent increases blood flow to the heart's arteries, helping identify by revealing perfusion defects under imaging modalities such as (SPECT) or cardiovascular magnetic resonance (CMR). The procedure typically involves intravenous administration of adenosine at doses of 140 μg/kg/min for 4-6 minutes, with imaging performed during infusion to assess myocardial ischemia. AMP acts as a metabolic to enhance the efficacy of antibiotics against resistant bacteria, such as methicillin-resistant Staphylococcus aureus (MRSA); studies show that AMP potentiates gentamicin's bactericidal effects by disrupting bacterial energy homeostasis, reducing minimum inhibitory concentrations by up to fourfold. For , low-dose adenosine compounds, which include AMP derivatives, have demonstrated potential in reducing mechanical through activation of adenosine A1 receptors in the peripheral and central nervous systems. Intrathecal or intravenous administration of these agents inhibits nociceptive transmission, providing relief in conditions like or post-surgical , with clinical trials reporting significant reductions in pain scores at doses around 50-100 μg without major systemic effects. This approach leverages adenosine's role in modulating neuronal excitability, offering an alternative to opioids in select refractory cases. Other therapeutic applications include the combination of with L-arginine for , where oral supplementation (e.g., 200 mg with 8 g L-arginine aspartate) promotes corpora cavernosa relaxation via pathway enhancement, improving International Index of Erectile Function scores in randomized trials. In -related conditions, administration induces a hypometabolic state that lowers oxygen demand by slowing mitochondrial respiration, thereby protecting neural tissues from ischemic damage in models of acute . This protective effect stems from 's activation of energy-sensing pathways like AMPK, which conserves cellular resources during low-oxygen states. Key contraindications for adenosine-based therapies, including those derived from AMP, include asthma or other bronchospastic conditions due to the risk of induced bronchoconstriction, and second- or third-degree heart block owing to potential exacerbation of atrioventricular conduction delays. Patients with these conditions require alternative diagnostic or therapeutic options to avoid adverse respiratory or cardiac events. Regarding regulatory status, the U.S. Food and Drug Administration (FDA) has approved intravenous for the acute termination of (PSVT) in adults and children, with rapid bolus dosing restoring in over 90% of cases within seconds. In contrast, AMP and its derivatives are primarily available as dietary supplements for immune support or energy enhancement, lacking broad pharmaceutical approvals for specific indications beyond investigational uses.

Recent research developments

Recent research has advanced the development of computational tools for identifying AMPK activators, with the 2025 introduction of MetaAMPK, a deep learning model employing meta-learners and bidirectional long-short-term memory networks to predict potential compounds for treating cancer, diabetes, and neurodegeneration. This framework achieves high accuracy in screening, facilitating the discovery of novel therapeutics by analyzing molecular features and reducing experimental costs. In post-stroke , AMP and AMPK signaling have been implicated in through enhanced and reduced , as highlighted in a 2025 review of ischemic injury mechanisms. Activation of AMPK following cerebral ischemia increases the AMP/ATP ratio, promoting autophagic processes that clear damaged cellular components and mitigate inflammatory responses in neurons and . A 2025 study demonstrated that AMP administration improves in mice by decreasing in , mediated via ecto-5'-nucleotidase (CD73) conversion to and subsequent ADORA2A receptor activation. This pathway enhances fat breakdown and corrects glucose-lipid dysregulation in high-fat diet models, offering insights into management. AMP has shown promise in combating antibiotic resistance, as a 2024 investigation revealed its synergistic enhancement of gentamicin's bactericidal activity against gentamicin-resistant by disrupting bacterial and TCA cycle function. Addressing research gaps, a 2025 review indicated emerging anti-aging benefits of GLP-1 receptor agonists (GLP-1RAs) in through synergy with AMPK activation, enhancing mitochondrial function and reducing age-related comorbidities like cardiovascular risk. AMPK modulation of fibrosis gained traction in 2024, with studies showing pharmacologic activation inhibits YAP/TAZ signaling in hepatic stellate cells, reducing deposition and progression in carbon tetrachloride-induced models.