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Hexene

Hexene is an with the molecular formula C₆H₁₂, belonging to the class of alkenes characterized by a six-carbon chain and one carbon-carbon . These hydrocarbons exist in multiple isomeric forms, including positional isomers such as , 2-hexene, and 3-hexene, as well as stereoisomers (E and Z configurations for 2-hexene and 3-hexene), with additional branched and cyclic variants possible under the same formula. The term "hexene" most commonly refers to these straight-chain linear alkenes, which are colorless liquids at , insoluble in , and highly flammable due to their unsaturated structure. Among the isomers, (also known as hex-1-ene) is the most industrially prominent, produced on a large scale as a linear alpha-olefin through the selective oligomerization of using catalysts like triethylaluminum, followed by . It serves primarily as a comonomer in the of to produce (LLDPE) and (HDPE), enhancing the flexibility, strength, and clarity of plastic films, pipes, and packaging materials. Other applications include its use as a , , and intermediate in synthesizing flavors, perfumes, dyes, and resins. Hexenes exhibit typical reactivity, undergoing addition reactions with , , and oxidizers, and they pose safety risks as flammable liquids with vapors heavier than air, potentially causing eye and skin irritation or upon exposure. In the United States, a major producer, annual production of exceeds one billion pounds (as of 2024), driven by demand in the sector.

Overview

Definition and general characteristics

Hexene refers to a class of organic compounds that are with the molecular formula C₆H₁₂, characterized by a carbon chain of six atoms containing exactly one carbon-carbon . This structure distinguishes hexenes from their saturated counterparts, the hexanes (C₆H₁₄), as the double bond introduces unsaturation into the skeleton. The general representation includes linear and branched chain variants where the double bond can occupy different positions along the chain, but all share the fundamental feature of a single C=C linkage amid the six-carbon framework. Hexenes are classified as olefins, a term historically used for alkenes due to their oily appearance and reactivity, and they belong to the broader family of unsaturated hydrocarbons. The for these compounds is calculated using the formula (2C + 2 - H)/2, where C is the number of carbon atoms and H is the number of atoms; for C₆H₁₂, this yields (2 \times 6 + 2 - 12)/2 = 1, confirming one unit of unsaturation consistent with a single or equivalent ring structure, though hexenes specifically feature the former. Hexenes were first synthesized in the through methods such as of alcohols or elimination reactions, reflecting early advances in during that era. Their industrial relevance, however, expanded significantly in the with the development of techniques, particularly following the of Ziegler-Natta catalysts in the , which enabled the of polyolefins like . In total, there are 13 constitutional isomers of hexene, encompassing various linear and branched configurations without including cyclic forms.

Industrial importance

Hexenes, particularly , play a pivotal role in the industry as comonomers in the production of (LLDPE), where they enhance the 's flexibility, tensile strength, and overall mechanical properties compared to traditional homopolymers. This incorporation allows for tailored material characteristics essential for films, bags, and containers, making LLDPE a cornerstone of modern plastics manufacturing. Global production of hexenes reached approximately 2.16 million metric tons in 2024, with accounting for the vast majority due to its dominance in LLDPE applications. This output reflects the compound's strategic importance, supported by major producers expanding capacities to meet rising demand. Beyond polymers, hexenes serve as key intermediates in the synthesis of specialty chemicals, including derived from processes and synthetic lubricants that provide superior and stability. These applications contribute to sectors like personal care and industrial cleaning, where hexene-based products offer enhanced performance. Market demand for hexenes is propelled by the and automotive industries, which rely on LLDPE for lightweight components and durable wraps, with projections indicating sustained growth through 2025 amid initiatives for recyclable and bio-based plastics. This trend underscores hexenes' alignment with goals, as advanced copolymers reduce material usage while maintaining functionality.

Nomenclature and isomers

Naming conventions

Hexenes are named according to the systematic rules for alkenes developed by the International Union of Pure and Applied Chemistry (IUPAC). The parent chain is the longest continuous carbon chain containing the , denoted by replacing the "-ane" ending of the corresponding with "-ene". The chain is numbered starting from the end that gives the carbons the lowest possible locants, prioritizing the first carbon of the . For terminal alkenes, this yields names such as hex-1-ene for the structure CH₂=CHCH₂CH₂CH₂CH₃. When the is internal, the position is specified similarly, and geometric (stereoisomeric) configurations are indicated using either the cis/trans or E/Z descriptors. The cis/trans system applies to disubstituted alkenes where the substituents are identical in type, with "cis" denoting substituents on the same side of the and "trans" on opposite sides; for more complex cases, the E/Z system uses Cahn-Ingold-Prelog priority rules to assign (E) for opposite high-priority groups and (Z) for same-side. Examples include cis-2-hexene and trans-2-hexene for CH₃CH=CHCH₂CH₂CH₃, or equivalently (Z)-hex-2-ene and (E)-hex-2-ene. For branched hexenes, the longest chain including the is selected as the parent, with branches (s like methyl) named and assigned the lowest possible locants after ensuring the double bond receives the lowest number. If choices exist, the chain is chosen to minimize locants overall. A representative example is 2-methylpent-1-ene, where the parent is pent-1-ene with a methyl at carbon 2. These conventions apply across the 13 constitutional isomers of hexene. Historically, alkenes were often designated by trivial names based on natural sources or simple descriptors, such as "amylene" for pentenes, leading to inconsistencies. The transition to systematic IUPAC naming accelerated in the mid-20th century, formalized by the 1957 IUPAC recommendations on organic nomenclature, which emphasized logical, reproducible naming to support global scientific collaboration.

Types of isomers

Hexene, with the molecular formula C₆H₁₂, displays a variety of constitutional isomers due to different positions of the carbon-carbon double bond and branching patterns in the hydrocarbon chain. These constitutional isomers further give rise to stereoisomers, primarily through geometric isomerism in cases where the double bond is internal and disubstituted with different groups on each carbon. The straight-chain constitutional isomers consist of three positional variants: 1-hexene, 2-hexene, and 3-hexene. While 1-hexene lacks geometric isomerism, both 2-hexene and 3-hexene exhibit E/Z (or cis/trans) configurations, resulting in a total of five stereoisomers for the linear hexenes. The branched constitutional isomers number ten, arising from various methyl or ethyl substitutions that maintain the C₆H₁₂ formula while introducing asymmetry in the carbon skeleton. Examples include 2-methyl-1-pentene, 3-methyl-1-pentene, and 2-methyl-2-pentene, among others. These branched forms contribute additional structural diversity, with some exhibiting geometric isomerism (e.g., in 3-methyl-2-pentene and 4-methyl-2-pentene) and others featuring chiral centers that allow for optical isomerism (e.g., in 3-methyl-1-pentene). However, most hexene isomers are achiral, lacking optical activity unless a stereogenic center is present. Stereoisomerism in hexene primarily manifests as geometric isomerism for alkenes with trisubstituted or tetrasubstituted double bonds where rotation is restricted, leading to distinct and forms based on the priority of substituents according to Cahn-Ingold-Prelog rules. Optical isomerism occurs only in those rare cases with a chiral carbon atom, such as an bearing four different groups, but the majority of hexene stereoisomers are achiral and do not exhibit enantiomerism. In total, the constitutional isomers yield 18 stereoisomers when accounting for both geometric and optical variants. The following table lists the 13 constitutional isomers, with text-based structural representations, corresponding CAS registry numbers (for the parent compound or representative stereoisomer where applicable), and the number of associated stereoisomers.
Constitutional IsomerStructural RepresentationCAS NumberNumber of Stereoisomers
1-HexeneCH₂=CH-CH₂-CH₂-CH₂-CH₃592-41-61
2-HexeneCH₃-CH=CH-CH₂-CH₂-CH₃592-43-82 (E/Z)
3-HexeneCH₃-CH₂-CH=CH-CH₂-CH₃693-87-82 (E/Z)
2-Methyl-1-penteneCH₂=C(CH₃)-CH₂-CH₂-CH₃565-47-91
3-Methyl-1-penteneCH₂=CH-CH(CH₃)-CH₂-CH₃760-20-32 (R/S)
4-Methyl-1-penteneCH₂=CH-CH₂-CH₂-CH(CH₃)₂691-37-21
2-Methyl-2-penteneCH₃-C(CH₃)=CH-CH₂-CH₃625-27-41
3-Methyl-2-penteneCH₃-CH=C(CH₃)-CH₂-CH₃922-62-32 (E/Z)
4-Methyl-2-penteneCH₃-CH=CH-CH(CH₃)-CH₃4461-48-72 (E/Z)
2-Ethyl-1-buteneCH₂=C(CH₂CH₃)-CH₂-CH₃513-35-91
3,3-Dimethyl-1-buteneCH₂=CH-C(CH₃)₂-CH₃558-37-21
2,3-Dimethyl-1-buteneCH₂=C(CH₃)-CH(CH₃)-CH₃563-78-01
2,3-Dimethyl-2-butene(CH₃)₂C=C(CH₃)₂563-79-11

Physical properties

Thermodynamic properties

Hexene isomers exhibit boiling points in the range of 60–70 °C, with linear terminal alkenes like having the lowest values due to reduced and surface area compared to internal or branched isomers. For instance, boils at 63.4 °C, while (E)-2-hexene boils at 68 °C and (Z)-3-hexene at 66.8 °C; branched isomers such as 2-methyl-1-pentene have boiling points around 62 °C, though some show slightly elevated values influenced by branching that increases intermolecular forces in less symmetric structures. Melting points for hexene isomers are generally low, ranging from -140 °C to -100 °C, reflecting their nonpolar and weak van der Waals interactions. Cis isomers typically have lower melting points than their trans counterparts due to less efficient molecular packing in the solid state; for example, melts at -139.7 °C, (E)-2-hexene at -133.3 °C, and (Z)-3-hexene at approximately -137 °C. The for hexene isomers is approximately 4,000 kJ/, with minor variations attributable to differences in isomer stability; more stable isomers, such as configurations, release slightly less due to lower energies. This value, calculated from enthalpies of formation (e.g., Δ_f H° = -73 kJ/ for liquid ), underscores the similar energetic content across isomers, as yields CO₂ and H₂O with comparable overall exothermicity. Vapor pressure and phase behavior of hexene isomers follow trends described by the Clausius-Clapeyron equation, which relates to (typically 30–32 kJ/mol) and temperature, indicating similar volatility profiles despite boiling point differences. For , the parameters (log_{10} P = 3.99063 - 1152.971 / (T - 47.301), with P in bar and T in K) predict pressures around 183 mmHg at 25 °C, with internal isomers showing marginally lower due to higher boiling points.

Spectroscopic and optical properties

Hexenes exhibit densities typically ranging from 0.66 to 0.70 g/cm³ at 20°C, with terminal alkenes like showing lower values around 0.673 g/cm³ due to their linear structure and reduced branching compared to internal isomers such as (E)-2-hexene at approximately 0.687 g/cm³. These compounds are insoluble in , with solubility for measured at about 0.05 g/L at 25°C, reflecting their nonpolar nature; however, they are miscible with common organic solvents such as , , , and . The of hexenes falls between 1.37 and 1.40 at 20°C, for instance 1.384 for , which serves as a practical metric for assessing sample purity and isomer composition in analytical settings. In () spectroscopy, hexenes display characteristic absorptions for the , including a C=C stretching band at approximately 1640–1660 cm⁻¹ and =C–H stretching vibrations between 3000 and 3100 cm⁻¹; for specifically, the C=C stretch appears near 1660 cm⁻¹. Proton nuclear magnetic resonance (¹H NMR) spectra of hexenes feature signals for vinylic protons (=CH) in the 4.5–6.5 ppm range downfield from (TMS), with the terminal =CH₂ protons of typically appearing as multiplets around 4.9–5.9 ppm, distinguishing the double bond from alkyl chain protons at 0.8–2.5 ppm.

Chemical properties

General reactivity

Hexenes, as alkenes, exhibit characteristic reactivity centered on the carbon-carbon , which serves as a nucleophilic site for various transformations. The π electrons of the render it electron-rich, facilitating reactions with species such as hydrogen halides (H-X), where the addition follows : the hydrogen attaches to the carbon atom bearing more hydrogens, while the halide bonds to the other carbon, leading to the more stable intermediate. Similar governs additions of like Br₂, forming vicinal dihalides via a intermediate, and under acidic conditions, yielding alcohols with Markovnikov orientation. This also enables mechanisms, such as anti-Markovnikov addition of HBr in the presence of peroxides, where radicals initiate chain propagation by adding to the less substituted carbon. The polarity of the double bond further supports coordination chemistry, where the π system can bind to metals, enabling catalytic processes like or insertion reactions, though these are modulated by the isomer's substitution pattern. Among hexene isomers, reactivity in electrophilic additions correlates inversely with , which increases with alkyl substitution due to stabilizing the ground state and the resulting ; the order is branched (more substituted) > internal > internal > terminal, with configurations favored over due to lower steric repulsion. For instance, displays higher rates in certain electrophilic additions compared to more substituted internal isomers, reflecting its lower and greater accessibility at the terminal . Hexenes are also prone to oxidation at the , demonstrating sensitivity to oxidative agents. Treatment with peracids, such as m-chloroperoxybenzoic acid (mCPBA), yields epoxides via stereospecific syn addition, preserving the alkene's geometry in the three-membered ring product. Under milder conditions with cold, alkaline KMnO₄, hexenes form vicinal diols (glycols) through syn , where the cyclic intermediate hydrolyzes to the 1,2-diol without carbon-carbon bond cleavage. These reactions highlight the double bond's vulnerability to oxygen transfer, with rates influenced by the and steric factors of the specific .

Specific reactions

One key reaction of hexene isomers, particularly , is its use as a comonomer in with to produce (LLDPE). This process employs Ti-based catalysts supported on MgCl₂, activated by triethylaluminum (AlEt₃), where the involves the coordination of and monomers to the active Ti-alkyl species, followed by sequential migratory insertion into the Ti-C bond, leading to chains with branches from incorporation. The comonomer effect enhances activity and alters microstructure, with insertion occurring at multiple active sites on the catalyst surface. Olefin metathesis facilitates isomer interconversion among hexene variants using ruthenium-based Grubbs catalysts, enabling the redistribution of alkylidene groups across double bonds. For instance, the self-metathesis or cross-metathesis of internal hexene isomers like 2-hexene (RCH=CHCH₃, where R = C₃H₇) can yield terminal alkenes and other isomers, as exemplified by the reaction 2 RCH=CHCH₃ → RCH=CH₂ + RCH=CHC₂H₅, proceeding via metal carbene intermediates that undergo [2+2] cycloadditions and cycloreversions. This reaction is particularly useful for achieving equilibrium mixtures of hexene positional isomers under mild conditions with second-generation Grubbs catalysts. Hydrogenation of hexene isomers, such as , to n-hexane is efficiently catalyzed by (Pd/C) under mild conditions with hydrogen gas, involving the dissociative adsorption of H₂ and π-complexation of the on Pd sites, followed by stepwise hydrogen addition. The reaction is exothermic, with a standard change of approximately -125 kJ/mol. The of , known as the oxo process, converts it to using (CO/H₂) and rhodium-based catalysts, such as HRh(CO)(PPh₃)₃, often with ligands to promote toward the linear n- (over 90% selectivity under optimized conditions). The proceeds associatively: the rhodium adds to the forming an alkyl-rhodium , followed by CO coordination and migratory insertion to generate an acyl-rhodium species, which is then hydrogenated to release the and regenerate the catalyst. This process operates industrially at 100-150°C and 10-30 bar, with catalysts preferred over for higher activity and linearity in terminal s like .

Production methods

Industrial processes

The primary industrial production of hexenes, particularly , occurs through on-purpose processes involving the oligomerization of , which have largely supplanted older methods like wax cracking. These modern routes emphasize high selectivity to to meet demand as a comonomer in manufacturing. Key technologies focus on trimerization, where three molecules combine to form , using homogeneous or heterogeneous catalysts under controlled conditions of temperature, pressure, and . One prominent method is the ethylene trimerization process developed by , employing a chromium-based catalyst system. This converts ethylene gas into an olefinic product with approximately 99 wt% 1-hexene selectivity, minimizing byproducts such as hexene isomers and heavier oligomers. The reaction typically operates in a like at moderate temperatures (around 100–120°C) and pressures (30–50 bar), followed by for purification. Similar chromium-catalyzed trimerization is utilized by , achieving selectivities exceeding 90% to 1-hexene in commercial plants, with ongoing optimizations to enhance catalyst stability and reduce energy use. Another selective trimerization route is the AlphaHexol™ process, licensed by Axens from IFP Energies nouvelles (IFPEN), which produces high-purity (>99%) from using advanced catalytic formulations. This technology improves efficiency over traditional methods by incorporating solvent-free options and integrated separation, targeting reduced operational costs and environmental footprint. In contrast, Shell's Higher Olefins Process () involves non-selective oligomerization of with nickel-based catalysts, generating a broad distribution of linear alpha-olefins from which is extracted via ; while less targeted, it contributes significantly to overall supply through . A smaller portion of arises as a byproduct from operations, where heavier hydrocarbons yield minor amounts (typically less than 5% of the olefin stream) alongside primary products like and . This fraction is recovered through complex sequences in petrochemical refineries. Globally, major producers including , , and dominate the market, with total capacity estimated at around 2.5 million metric tons per year in 2025, driven by expansions in Asia and the to support growth.

Synthetic routes

Hexenes can be synthesized in settings through various organic transformations, providing alternatives to industrial-scale production methods. These routes are particularly useful for preparing specific isomers or isotopically labeled variants for research purposes. One common method for synthesizing involves the , where reacts with the derived from butyltriphenylphosphonium salt, specifically \ce{Ph3P=CH-CH2-CH2-CH2-CH3}, to form the terminal . This olefination proceeds via a phosphonium intermediate that attacks the of the , yielding and triphenylphosphine oxide as a byproduct. The reaction typically employs non-stabilized ylides under salt-free conditions to favor the Z-isomer, though can occur post-reaction. Another straightforward approach is the of 1-bromohexane using a strong base such as alcoholic (KOH). This E2 removes the bromine and an adjacent β-hydrogen, predominantly forming due to Hofmann product selectivity in primary alkyl halides under these conditions. The reaction is typically conducted by heating the alkyl bromide with ethanolic KOH, achieving high yields of the terminal while minimizing over-elimination or side products. Olefin metathesis offers a route to using catalysts like ruthenium-based Grubbs complexes. This redistribution of alkylidene fragments allows for the formation of the desired C6 , though practical implementations often involve self-metathesis of to generate 3-hexene as an intermediate, which can be further adjusted. The process avoids detailed mechanistic complexity in laboratory applications, focusing on catalyst loading and solvent effects for selectivity. For isomer-specific synthesis, trans-2-hexene can be prepared with E-selectivity through partial of 1,3-hexadiene using -based catalysts. This targets one of the conjugated double bonds, favoring the internal trans-alkene due to thermodynamic stability and catalyst surface interactions that promote syn-addition followed by . Supported on alumina, for instance, achieves high monoene selectivity even at moderate conversions, yielding predominantly (E)-2-hexene.

Applications and uses

Polymer industry

1-Hexene serves primarily as a comonomer in the production of (LLDPE) through copolymerization with , where it is incorporated at levels typically ranging from 2 to 10 mol% to introduce short-chain butyl branches that disrupt crystallinity and reduce density to around 0.915–0.925 g/cm³. These branches enhance the material's flexibility, tensile strength, and puncture resistance compared to homopolymer , making LLDPE suitable for applications such as stretch films and agricultural films. The incorporation occurs via statistical copolymerization, resulting in a random distribution of 1-hexene units along the chain during processes using metallocene or Ziegler-Natta catalysts. In (HDPE) production, is used in smaller amounts or blended with HDPE resins to improve processability, impact resistance, and optical clarity without significantly compromising the high crystallinity that defines HDPE's rigidity. Such blends facilitate easier and molding while enhancing clarity for packaging applications like bottles and pipes. The majority of industrial consumption is dedicated to , particularly LLDPE and HDPE, enabling the manufacture of durable films, pipes, and containers that dominate global markets. This high demand underscores 's critical role in tailoring properties for diverse end-use sectors.

Other industrial applications

Hexenes, particularly , serve as key intermediates in the production of through conversion routes that yield alcohols. In processes such as the Higher Olefin Process (), linear alpha olefins like are oligomerized from and then transformed into alcohols via followed by , enabling the synthesis of linear alkylbenzene sulfonates and ethoxylates used in and detergents. These benefit from the linear structure of hexene-derived alcohols, which enhances biodegradability and cleaning efficiency in formulations. In the lubricants sector, undergoes oligomerization to produce polyalphaolefins (PAOs), which form the base stocks for high-performance synthetic oils. This cationic or metallocene-catalyzed process yields low-viscosity PAOs with excellent thermal stability and low-temperature fluidity, suitable for automotive and industrial lubricants that outperform mineral oils in extreme conditions. For instance, oligomerization of with catalysts like Cp2ZrCl2 in the presence of methylaluminoxane produces dimers and trimers that, after , serve as viscosity index improvers in engine oils. Hexenes also contribute to fine chemicals via , where reacts with synthesis gas (CO/H2) over or catalysts to form heptanal and isoheptanal. These aldehydes are versatile intermediates in the synthesis of flavors, fragrances, and pharmaceutical precursors, such as those used in the production of vitamins and agrochemicals. The process achieves high selectivity for linear aldehydes, which are further oxidized or reduced to carboxylic acids and alcohols employed in perfumery and manufacturing. Branched hexene isomers, such as isohexene (2-methyl-1-pentene or 4-methyl-1-pentene), act as fuel additives to boost ratings in blending. These compounds, with research octane numbers exceeding 90, enhance efficiency and reduce engine knock when added to low-octane streams, providing a cleaner alternative to aromatic boosters. Their unsaturated branched structure allows effective integration into reformate without significantly altering .

Safety and environmental considerations

Health hazards

exhibits low via oral and dermal routes, with an oral LD50 greater than 5,600 mg/kg in rats and a dermal LD50 greater than 2,000 mg/kg in rabbits. It is not irritating to but may cause slight to the eyes upon direct contact, and vapors may cause to the , leading to symptoms such as coughing and wheezing. Inhalation of high concentrations can produce effects, including drowsiness, , , , and , with an LC50 of 40–110 mg/L (4 hours in rats). is classified as an aspiration hazard, potentially causing severe lung damage or fatality if swallowed and aspirated into the airways. Regarding carcinogenicity, 1-hexene is not classified as a human by the International Agency for Research on Cancer (IARC), the National Toxicology Program (NTP), or OSHA, with no components identified as probable, possible, or confirmed carcinogens in available evaluations. The American Conference of Governmental Industrial Hygienists (ACGIH) has established a (TLV) of 50 as an 8-hour time-weighted average for occupational exposure to prevent central nervous system impairment. No adverse reproductive or developmental effects were observed in rat screening studies (OECD Guideline 421) at doses up to 1,000 mg/kg. Repeated may also lead to liver, , and effects, with a (NOAEL) of 101 mg/kg in 28-day rat studies, but it is not classified as a specific target organ for repeated based on current . As a highly flammable liquid with a flash point of -26°C, 1-hexene poses significant fire and explosion risks during handling, requiring storage in cool, well-ventilated areas away from ignition sources and oxidizers. To prevent peroxidation upon exposure to air, it should be stored and handled under an inert atmosphere such as nitrogen, using explosion-proof equipment and non-sparking tools.

Environmental impact

Hexene, particularly , exhibits moderate biodegradability in aerobic conditions, with studies showing greater than 60% degradation within 28 days according to Test Guideline 301C. This classification as readily biodegradable indicates it does not persist long-term in under favorable microbial conditions, though safety data sheets confirm it is not considered persistent, bioaccumulative, or toxic (PBT) overall. In aquatic environments, 1-hexene demonstrates moderate toxicity to fish, with an LC50 value of 5.6 mg/L for rainbow trout (Oncorhynchus mykiss) over 96 hours. This level suggests potential harm to aquatic life at low concentrations, classifying it as toxic to aquatic organisms and prompting precautions in release scenarios. Under European regulations, 1-hexene is registered under REACH (Registration, Evaluation, Authorisation and Restriction of Chemicals) as part of the higher olefins category, requiring detailed safety assessments for environmental release. In the United States, it is listed on the TSCA (Toxic Substances Control Act) Inventory managed by the EPA, subjecting it to reporting and risk management requirements. As a volatile organic compound (VOC), emissions of 1-hexene are regulated under the Clean Air Act to control ozone formation, with limits on industrial releases to mitigate atmospheric impacts. Efforts toward include a growing shift in the 2020s to bio-based production of derived from renewable , often via to followed by oligomerization, reducing reliance on fossil feedstocks and lowering carbon footprints. This transition aligns with broader industry trends in bio-olefins, supported by advancements in catalytic processes to enable scalable, lower-emission .

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